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标准品/甲醇中4种香兰素混标/GB 5009.284-2021

¥520.00
81702b
1mL

甲醇中4种香兰素混标

CAS号名称标准值单位
121-33-5 香兰素 1000 μg/mL
120-14-9 甲基香兰素 1000 μg/mL
121-32-4 乙基香兰素 1000 μg/mL
91-64-5 香豆素 1000 μg/mL

 

 

 

 

甲醇中4种香兰素混标

Reference Material

This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025ISO 17034 and a registered quality management system ISO 9001.

 
Product Name(产品名称) 4 Vanillin Mix in Methanol,1000μg/mL(甲醇中4种香兰素混标)
 
Part Number(产品编号) 81702b
 
Lot Number(产品批号) -
 
Expiry Date(失效日期) 2024-Apr-10____________________________________________________
 
Storage(存储条件)           (-18±5)℃,Keep in the shade
                                                        冷冻(-18±5)℃,置于阴凉处
 
CERTIFIED
Component
No.
(组分数)
Peak
Sequence
(出峰顺序)
Component
(组分)
CAS No. Concentration
(μg/mL)
(浓度)
Relative Expanded
Uncertainty(%) (k=2)
(相对扩展不确定度)
1 1 Vanillin (香兰素) 121-33-5 1000 2
2 2 Methyl Vanilline (甲基香兰素) 120-14-9 1000 2
3 Ethyl Vanillin (乙基香兰素) 121-32-4 1000 2
4 3 Coumarin (香豆素) 91-64-5 1000 2

C H R O M A T O G R A M

 
 
 Instrument(检测仪器)  HPLC/DAD
 
 Column(色谱柱)  C18(3.0×100mm,2.7um)
 
 Column Oven(柱温)  35℃
 
 Wavelength(波长)  280nm
 
 Method Details(方法参数)
  A: 0.1% Phosphoric Acid(0.1% 磷酸)
  B: Acetonitrile(乙腈)
 
Time/min A/% B/%
0.00 90 10
0.50 90 10
4.00 10 90
8.00 10 90
8.10 90 10
12.00 90 10
 
Intended Use

This RM is intended for use in a laboratory as a calibration and quality control standard or in method development for analytical techniques.

Uncertainty

The certified value(s) and uncertainty(ies) are determined in accordance with ISO 17034 with an 95% confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including uncertainties of preparation, purity of neat materials, homogeneity, stability testing.

Traceability

The balances used for gravimetric measurements are calibrated with weights traceable to the national standards. The calibration of the balances is verified annually by an external accredited calibration service. This analysis method has been verified using an approach consistent with ISO 17034:2016 & ISO 17025:2017.

Homogeneity

Random replicate samples of the final packaged RM have been analysed to prove homogeneity consistent with ISO 17034.

Storage

The RM should be stored in the original sealed bottle at the indicated temperature.

 

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